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Article Dans Une Revue Solid State Nuclear Magnetic Resonance Année : 2009

Homonuclear dipolar decoupling schemes for fast MAS

Résumé

We present two one-dimensional methods that allow direct observation of highly resolved 1H spectra in solid-state NMR. The methods, which work mainly at 30–35 kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.

Domaines

Chimie

Dates et versions

hal-04559499 , version 1 (25-04-2024)

Identifiants

Citer

Jean-Paul Amoureux, Bingwen Hu, Julien Trebosc, Qiang Wang, Olivier Lafon, et al.. Homonuclear dipolar decoupling schemes for fast MAS. Solid State Nuclear Magnetic Resonance, 2009, Solid State Nuclear Magnetic Resonance, 35, pp.19-24. ⟨10.1016/j.ssnmr.2008.10.006⟩. ⟨hal-04559499⟩
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